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ONLINE HANDS ON TRAINING ON

RIETVELD REFINEMENT

(UsingĀ  FULLPROF And JANA Software)

(25 JAN- 02 FEB 2023)

DAY RESOURCE PERSON TOPICS
Day 1 Dr. Sudhindra Rayaprol
Rietveld Refinement Method using FullProf for Crystallographic Structures using Powder X-ray Diffraction Data
Day 2 Dr. Sudhindra Rayaprol  

  • Gathering information needed for refinement
  • Preparation of PCR file
  • Observing data files (DAT) file
  • Structural refinement using actual XRD data
  • Identifying single phase / multiphase from XRD data
  • Understanding the results
Day 3 Dr. Pradeep Reddy
  • XRD basics
  • Powder XRD data analysis
  • Identifying single phase / multiphase from XRD data
  • Introduction to MATCH Software

(How to use MATCH software, Phase identification using MATCH software, obtaining phase information of the sample, advanced option in the MATCH software, etc)

Day 4 Dr. Pradeep Reddy
  • Introduction to the Powder cell
  • Advantages of powder cell
  • Le Bail Fitting
  • Gathering information needed for refinement
  • Preparation of PCR file
  • Structural refinement using actual XRD data – Rietveld Refinement on powder XRD data of single-phase samples (Perovskites/Metal Oxides/ nano particles) using FullProf
  • Understanding the results
Day 5 Dr. Pradeep Reddy  

Rietveld Refinement on powder XRD data of multiphase sample (Perovskites/Metal Oxides/ nano particles/Alloys) using FullProf

  • Identifying single phase / multiphase from XRD data
  • Adding additional phases
  • Carrying out multiphase refinement
  • Understanding the results
DayĀ  6 Dr. Pradeep Reddy
  • Rietveld Refinement on powder XRD data of various samples
  • Analyzing the various results obtained from the Rietveld refinement
  • Drawing the crystal structure
  • Bond lengths, bond angles etc.
Day 7Ā  Dr. Shivani Sharma
  • The powder X-ray refinement using FullProf
  • Carrying out single/multiphase refinement
  • Understanding the results
Day 8 Dr. Shivani Sharma
  • Neutron diffraction data refinement using FullProf
  • Carrying out single/multiphase refinement
  • Understanding the results
Day 9 Dr. Shivani Sharma
  • Lebail fit and Rietveld refinement of Powder X-ray Diffraction data using JANA
  • Magnetic structure refinement using JANA software

Resource Person

 

Dr. Sudhindra Rayaprol is working as Scientist ā€“ G at UGC-DAE Consortium for Scientific Research, Mumbai Centre since 2006. He completed his Ph.D. from Saurashtra University, Rajkot in 2003 and postdoctoral research from the Tata Institute for Fundamental Research, Mumbai in 2005. He has received the prestigious Alexander von Humboldt Research Fellowship and worked as researcher at Institute fur Anorganische und Analytische Chemie, Universitat MĆ¼nster, Germany from 2005-2006. He was also awarded N. S. Satyamurthy Memorial Award in Physics for Young Scientists for the year 2010 given by Indian Physics Association and Young Achiever Award in the DAE – Solid State Physics Symposium ā€“ 2011.

 

Ā  Dr. Shivani Sharma is currently working as a Research Associate in Brookhaven National Laboratory, USA. She was a post-doctoral fellow at National High Magnetic Field Lab, Florida state University, Florida, USA since December 2019. Ā She has received DST Inspire faculty award in material science in July-2017 and worked as DST Inspire Faculty at Indian Institute of Science Education and Research, Bhopal, January 2018 ā€“ March 2018. She completed her Ph.D. from UGC-DAE Consortium for Scientific Research, Indore in 2017. Her research interest includes material synthesis (polycrystal and single crystal using melt growth, bridgeman, flux growth etc., structural characterization using X-rays, physical properties measurements using PPMS and MPMS, Structural characterization using 25 T DC field based XRD setup.

Dr. Pradeep Reddy Vanga is working as an Assistant Professor in Vel Tech Rangarajan Dr. Sagunthala R&D Institute of Science and Technology, Chennai in School of Science and Humanities since 2017. He completed his M.Sc from Pondicherry University and Ph.D. from NIT Trichy. He is having more than 15 research articles in the international peer reviewed journals. His research work is focused on Multiferroics and Photocatalysis.

COURSE FEE: Rs. 2000/

 

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Ā  Ā  Ā  Ā  Ā CLICK HERE TO REGISTER
  • Cost
    ā‚¹2000.00
  • Start Time
    January 25 - 7:00pm
  • End Time
    February 2 - 8:30pm
  • Phone
    +91 9605241561
  • Email
    director@thesias.in
  • Organizer
    SIAS

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